pilot-scale glass reactor with adjustable speed and heating

Pilot-scale glass reactor is a multifunctional reaction system designed for reaction process amplification and process optimization, which is widely used in the fields of new material synthesis, drug development, chemical pilot test and natural product extraction.

Description

Pilot-Scale Glass Reactor

The pilot-scale glass reactor is designed for precise control of temperature, pressure, and stirring in scale-up chemical processes. Serving as a bridge between laboratory research and industrialized production, this equipment is ideal for pharmaceutical, chemical, bioengineering, materials, and environmental applications.

Main Features

  1. Reaction Vessel: Made of 3.3 borosilicate glass for superior thermal shock resistance and acid/alkali corrosion resistance, ensuring long-term safe operation.
  2. Wide Working Conditions: Temperature range from -80°C to 200°C; pressure range from 0 to -0.1MPa, suitable for low-temperature synthesis and decompression reactions.
  3. Optimized Pipeline Design: Jacket interface uses stainless steel insulated hoses to prevent interface stress damage from thermal cycling.
  4. High Sealing Stirring System: Sealed bearings ensure smooth operation and prevent impurity entry into the reaction system.
  5. Anticorrosive Components: PTFE stirring blades and PTFE-coated stainless steel shaft combine mechanical strength and chemical stability.
  6. Movable Bracket: Stainless steel and aluminum alloy spray frame, neat and corrosion-resistant, with brake wheels for easy positioning and cleaning.
  7. Safe Discharge Design: Inclined, non-accumulating discharge valve at the top reduces residue, simplifies collection and post-processing.
  8. Convenient Data Monitoring: Digital display and vacuum gauge for real-time temperature, stirring speed, and system pressure monitoring.
  9. Structural Protection: External circulation pipe fixed to frame, avoiding glass interface stress and extending service life.

Working Principle

  1. Double-layer jacket allows heat/cold source (thermal oil, water, ethanol) to circulate, controlled by external thermostat; insulated hose connections prevent glass stress for stable temperature control.
  2. Motor-driven stirring shaft creates effective mixing, solid suspension, and uniform heat transfer; blade shapes selectable for different fluid characteristics; pressure monitored by vacuum gauge for vacuum or atmospheric operation.
  3. Inclined bottom discharge port enables smooth, residue-free material discharge and easy cleaning after reaction.

Application Areas

  1. Pharmaceutical Industry: API synthesis, crystal screening, impurity reaction assessment.
  2. Fine Chemical Industry: Development of flavors, dyes, additives, catalysts, high-value products.
  3. Organic Synthesis Research: Condensation, cyclization, redox, coordination reactions.
  4. Bioengineering: Enzyme reactions, cell extraction, optimization of organic acid or polysaccharide synthesis.
  5. New Material Development: Synthesis of nanoparticles, polymers, MOFs, and high-performance materials.
  6. University Research Platform: Reaction process scale-up, pilot demonstrations, teaching.
  7. Environmental Engineering: Reactivity testing, water treatment additive optimization, experimental program development.
Technical Parameters
pilot-scale glass reactor with adjustable speed and heating
ModelTR-10TR-10ExTR-20TR-20ExTR-50TR-50Ex
Vessel volume10L20L50L
Jacket volume8L3L9L6L13L16L
Funnel volume1.0L2.0L2L
Operating pressureOrdinary or negative pressure
Working temperature-80°C to 200°C
Condenser cooling area0.234 square meters0.341 square meters0.265 square meters0.429 square meters
Stirring speed20rpm to 500rpm50rpm to 500rpm20rpm to 500rpm50rpm to 500rpm20rpm to 500rpm50rpm to 500rpm
Power supply100-240V, 50/60Hz220-240V, 50/60Hz100-240V, 50/60Hz220-240V, 50/60Hz100-240V, 50/60Hz220-240V, 50/60Hz
Drain port, ground clearance320mm320mm355mm320mm
Dimensions(WxDxH)845x640x1780mm845x640x1910mm870x580x1910mm900*690*2100mm900x690x2050mm
pilot-scale glass reactor with adjustable speed and heating
ModelTR-100TR-100Ex
Vessel volume100 L
Jacket volume25 L30L
Feeding flask volume10 L
Receiving flask volume20 L
Glass materialHigh borosilicate glass 3.3
Frame and connection parts materialSUS304 + aluminum plate sprayingSUS304
Operating pressureOrdinary or negative pressure
Working temperature-80°C to 200°C
Condenser cooling area0.954 square meters
Stirring speed20rpm to 500rpm50rpm to 500rpm
Power supply100-240V, 50/60Hz220-240V, 50/60Hz
Drain port ground clearance340mm
Dimensions(WxDxH)1270x810x2360mm1200x790x2360mm