pilot-scale glass reactor with adjustable speed and heating

Pilot-scale glass reactor is a multifunctional reaction system designed for reaction process amplification and process optimization, which is widely used in the fields of new material synthesis, drug development, chemical pilot test and natural product extraction.

Description

Pilot-Scale Glass Reactor

The pilot-scale glass reactor is designed for precise control of temperature, pressure, and stirring in scale-up chemical processes. Serving as a bridge between laboratory research and industrialized production, this equipment is ideal for pharmaceutical, chemical, bioengineering, materials, and environmental applications.

Main Features

  1. Reaction Vessel: Made of 3.3 borosilicate glass for superior thermal shock resistance and acid/alkali corrosion resistance, ensuring long-term safe operation.
  2. Wide Working Conditions: Temperature range from -80°C to 200°C; pressure range from 0 to -0.1MPa, suitable for low-temperature synthesis and decompression reactions.
  3. Optimized Pipeline Design: Jacket interface uses stainless steel insulated hoses to prevent interface stress damage from thermal cycling.
  4. High Sealing Stirring System: Sealed bearings ensure smooth operation and prevent impurity entry into the reaction system.
  5. Anticorrosive Components: PTFE stirring blades and PTFE-coated stainless steel shaft combine mechanical strength and chemical stability.
  6. Movable Bracket: Stainless steel and aluminum alloy spray frame, neat and corrosion-resistant, with brake wheels for easy positioning and cleaning.
  7. Safe Discharge Design: Inclined, non-accumulating discharge valve at the top reduces residue, simplifies collection and post-processing.
  8. Convenient Data Monitoring: Digital display and vacuum gauge for real-time temperature, stirring speed, and system pressure monitoring.
  9. Structural Protection: External circulation pipe fixed to frame, avoiding glass interface stress and extending service life.

Working Principle

  1. Double-layer jacket allows heat/cold source (thermal oil, water, ethanol) to circulate, controlled by external thermostat; insulated hose connections prevent glass stress for stable temperature control.
  2. Motor-driven stirring shaft creates effective mixing, solid suspension, and uniform heat transfer; blade shapes selectable for different fluid characteristics; pressure monitored by vacuum gauge for vacuum or atmospheric operation.
  3. Inclined bottom discharge port enables smooth, residue-free material discharge and easy cleaning after reaction.

Application Areas

  1. Pharmaceutical Industry: API synthesis, crystal screening, impurity reaction assessment.
  2. Fine Chemical Industry: Development of flavors, dyes, additives, catalysts, high-value products.
  3. Organic Synthesis Research: Condensation, cyclization, redox, coordination reactions.
  4. Bioengineering: Enzyme reactions, cell extraction, optimization of organic acid or polysaccharide synthesis.
  5. New Material Development: Synthesis of nanoparticles, polymers, MOFs, and high-performance materials.
  6. University Research Platform: Reaction process scale-up, pilot demonstrations, teaching.
  7. Environmental Engineering: Reactivity testing, water treatment additive optimization, experimental program development.
Technical Parameters
pilot-scale glass reactor with adjustable speed and heating
Model TR-10 TR-10Ex TR-20 TR-20Ex TR-50 TR-50Ex
Vessel volume 10L 20L 50L
Jacket volume 8L 3L 9L 6L 13L 16L
Funnel volume 1.0L 2.0L 2L
Operating pressure Ordinary or negative pressure
Working temperature -80°C to 200°C
Condenser cooling area 0.234 square meters 0.341 square meters 0.265 square meters 0.429 square meters
Stirring speed 20rpm to 500rpm 50rpm to 500rpm 20rpm to 500rpm 50rpm to 500rpm 20rpm to 500rpm 50rpm to 500rpm
Power supply 100-240V, 50/60Hz 220-240V, 50/60Hz 100-240V, 50/60Hz 220-240V, 50/60Hz 100-240V, 50/60Hz 220-240V, 50/60Hz
Drain port, ground clearance 320mm 320mm 355mm 320mm
Dimensions(WxDxH) 845x640x1780mm 845x640x1910mm 870x580x1910mm 900*690*2100mm 900x690x2050mm
pilot-scale glass reactor with adjustable speed and heating
Model TR-100 TR-100Ex
Vessel volume 100 L
Jacket volume 25 L 30L
Feeding flask volume 10 L
Receiving flask volume 20 L
Glass material High borosilicate glass 3.3
Frame and connection parts material SUS304 + aluminum plate spraying SUS304
Operating pressure Ordinary or negative pressure
Working temperature -80°C to 200°C
Condenser cooling area 0.954 square meters
Stirring speed 20rpm to 500rpm 50rpm to 500rpm
Power supply 100-240V, 50/60Hz 220-240V, 50/60Hz
Drain port ground clearance 340mm
Dimensions(WxDxH) 1270x810x2360mm 1200x790x2360mm